Shipping Samples

1. Samples can be shipped directly in the GCMS vial that they will be analysed in. Suitable vials are Fisherbrand 2 mL Clear Vial PTFE/SIL Cat. No. 03-391-15 with GCMS caps, Fisherbrand 9mm Blue Cap T/S Cat. No 03-391-14

2. When shipping the vials be sure to a) mark the level of the solvent on the vial, b) wrap vials with parafilm, and label them

3. The solvent carrier must comply with the United States Center for Disease Control (CDC) and United States Department of Agriculture (USDA) as being non-etiologic (biologically active). The samples must further comply with a variety of environmental regulations (Toxic Substances Control Act (TSCA)) which are laid out by the United States Environmental Protection Agency (US EPA).

4. A searchable database which lists TSCA restrictions on a variety of compounds is available at Cornell University. This data base lists whether or not the compound is unknown, variable, complex, and biological (UVCB) or a known regulated material. It also gives the Chemical Abstracts (CAS) chemical registration number and formula.

5. The shipping company may have a specific form that must be filled out. The DHL shipping form requests statement of TSCA applicability, CAS number and forumla.

6. A form letter from Alanah Fitch specifying that the sample is part of a scientific project for analysis of water samples, with the solvent carrier, and the non-etiologic label can be obtained by contacting Alanah Fitch (afitch@luc.edu) at the time that you are arranging for time on the GC-MS.

7. Shipping generally takes 1-2 weeks, depending on whether the sample gets derailed in New York for TSCA compliance check. The cost of shipping approximately 50 vials is $50 (DHL) and the cost is borne by the GLIC consortium.

 

Workshop Information

Fisherbrand vials

USEPA TSCA information

Cornell TSCA searchable database

Shipping Form (TSCA)

DHL Africa

Great Lakes Instrumentation Collaboratory: Sharing Chemical Instrumentation Globally for Research and Education, Est. 2004

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Page Modified: July 25, 2007
  1. Use of Organo Chlorine Pesticides
  2. Toxicology of OrganoChlorine Pesticides
  3. Endocrine Disruptors
  4. Risk Assessment of OCP
  5. Water Treatment and Sampling
  6. Environmental Chemistry of OCP
  7. Chemistry of Sample Prep.
  8. Landscape Sampling
  9. US EPA Method for OCP
  10. Gas Chromatography
  11. Mass Spectra of OC standards
  12. Step by Step Creation of Methods File
  13. Trace MS methods development
  14. Parent Ion Spectra
  15. Instrument Design
  16. Chemometrics
  17. Spatial Interpolation of Data
  18. Background on Remote Control
  1. Become a GLIC Member
  2. Read Content Modules 10-15
  3. Pass an On-Line Quiz
  4. Schedule a Training Experiment
  5. Download Virtual Private Network
  6. Access GCMS computer
  7. Run a Training Experiment
  8. Analyze Mass Spectra of Training Experiment Unknown
  9. Schedule the GCMS for your Experiment
  10. Prepare Your Samples
  11. Ship Your Samples
  12. Access the GCMS computer
  13. Upload your Excel Sample Data
  14. Open the Template Sequence File
  15. Run Your Experiment